THE TREATMENT AND DISPOSAL OF DYE-CONTAMINATED WASTEWATER IS ONE OF THE MOST SERIOUS ENVIRONMENTAL PROBLEMS FACED BY THE TEXTILE. MANY TREATMENT METHODS HAVE BEEN DEVELOPED TO REMOVE DYES FROM WASTEWATER. THESE TREATMENT METHODS CAN BE DIVIDED INTO PHYSICAL, CHEMICAL AND BIOLOGICAL SCHEMES. ALTHOUGH CHEMICAL AND BIOLOGICAL APPROACHES ARE EFFECTIVE IN REMOVING DYES, THEY REQUIRE SPECIAL EQUIPMENT AND ARE USUALLY ENERGY INTENSIVE, ADDITIONALLY, THESE PROCESSES OFTEN GENERATE LARGE AMOUNTS OF BYPRODUCTS. AMONG ALL EXISTING TECHNIQUES, ADSORPTION IS CONSIDERED THE MOST EFFICIENT AND ECONOMY .IN THIS STUDY, PREPARATION OF POLYANILINE (PANI) AND ITS NANOCOMPOSITE CONTAINING SBA-15 WAS DISCUSSED, AND THEIR CAPABILITY TO REMOVAL OF REACTIVE ORANGE 16 (RO16) FROM AQUEOUS SOLUTION WAS STUDIED. POLYANILINE (PANI) SYNTHESIZED CHEMICALLY IN THE PRESENCE OF POTASSIUM IODATE (KIO3) AS AN OXIDANT AND COATED ON SBA-15. THE REMOVAL OF RO16 WAS INVESTIGATED USING PANI, AND PANI/SBA-15 NANOCOMPOSITE, RESPECTIVELY. THE PRODUCTS WERE INVESTIGATED IN TERMS OF MORPHOLOGY AND CHEMICAL STRUCTURE WITH SCANNING ELECTRON MICROSCOPY (SEM) AND FOURIER-TRANSFORM INFRARED SPECTROSCOPY (FTIR), RESPECTIVELY. BATCH STUDIES WERE PERFORMED TO EVALUATE THE INFLUENCE OF VARIOUS EXPERIMENTAL PARAMETERS LIKE PH, ADSORBENT DOSAGE AND CONTACT TIME. OPTIMUM CONDITIONS FOR RO16 REMOVAL WERE FOUND TO BE PH 2, ADSORBENT DOSAGE OF 0.5 G/L, EQUILIBRIUM TIME 60 MIN.